All samples containing carbon nanotubes showed similar XRD patterns after dehydrogenation. There is no residual hydride, which indicates that complete hydrogen has been released (Figure 4a). Figure 4b shows that both magnesium and magnesium hydroxide are present in the sample containing 5wt% graphene+2ml cyclohexane. It is inferred that the activation conditions in the experiment have less effect on the complete reduction of the alloy oxide layer than this additive. Research shows that high temperature can effectively reduce the oxide layer on the surface of magnesium alloy. The formation of oxide and hydroxide layers on the alloy surface greatly reduces the hydrogen absorption capacity. The same is true for other organic additives and hydrogenation conditions.
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